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水(shui)熱合成反應釜的工藝詳細篇

水(shui)熱(re)(re)合(he)成反(fan)(fan)(fan)(fan)應釜(fu)在加(jia)熱(re)(re)進行時(shi)會遇到空(kong)氣里的(de)(de)(de)水(shui)氣,適應溫(wen)(wen)(wen)(wen)(wen)度(du)控(kong)制(zhi)(zhi)(zhi)系(xi)(xi)統在控(kong)制(zhi)(zhi)(zhi)工藝(yi)（如(ru)化學(xue)反(fan)(fan)(fan)(fan)應工藝(yi)）的(de)(de)(de)過程中，持續不斷的(de)(de)(de)調節PID參(can)數(shu)來給(gei)予工藝(yi)zui好的(de)(de)(de)控(kong)制(zhi)(zhi)(zhi)溫(wen)(wen)(wen)(wen)(wen)度(du)和(he)(he)響應時(shi)間，這種(zhong)過程是通(tong)過有(you)效的(de)(de)(de)多方(fang)(fang)位的(de)(de)(de)測定(ding)(ding)溫(wen)(wen)(wen)(wen)(wen)度(du)，溫(wen)(wen)(wen)(wen)(wen)度(du)變(bian)化和(he)(he)溫(wen)(wen)(wen)(wen)(wen)度(du)變(bian)化的(de)(de)(de)速率(lv)來實現的(de)(de)(de). 水(shui)熱(re)(re)合(he)成反(fan)(fan)(fan)(fan)應釜(fu)高(gao)壓(ya)消解罐(guan)是一(yi)種(zhong)能(neng)(neng)分解難(nan)溶物(wu)質(zhi)(zhi)的(de)(de)(de)密閉(bi)容器(qi).可用(yong)于(yu)原子吸收光(guang)譜及(ji)等(deng)離(li)(li)子發射(she)等(deng)分析中的(de)(de)(de)溶樣(yang)預(yu)處(chu)(chu)理,也可用(yong)于(yu)小(xiao)劑量的(de)(de)(de)合(he)成反(fan)(fan)(fan)(fan)應.還可利用(yong)罐(guan)體(ti)內強(qiang)酸(suan)或強(qiang)堿且(qie)高(gao)溫(wen)(wen)(wen)(wen)(wen)高(gao)壓(ya)密閉(bi)的(de)(de)(de)環境(jing)來達到快速消解難(nan)溶物(wu)質(zhi)(zhi)的(de)(de)(de)目的(de)(de)(de).在氣相、液相、等(deng)離(li)(li)子光(guang)譜質(zhi)(zhi)譜、原子吸收和(he)(he)原子熒光(guang)等(deng)化學(xue)分析方(fang)(fang)法中做樣(yang)品前處(chu)(chu)理. 水(shui)熱(re)(re)合(he)成反(fan)(fan)(fan)(fan)應釜(fu)的(de)(de)(de)操作(zuo)方(fang)(fang)法,將(jiang)反(fan)(fan)(fan)(fan)應物(wu)系(xi)(xi)指與(yu)釜(fu)體(ti)內,并保(bao)證加(jia)料(liao)系(xi)(xi)數(shu)小(xiao)于(yu)0.8.當(dang)反(fan)(fan)(fan)(fan)應物(wu)系(xi)(xi)有(you)腐蝕性時(shi)要將(jiang)其(qi)置于(yu)四氟襯(chen)套內,方(fang)(fang)可保(bao)證釜(fu)體(ti)不受腐蝕.將(jiang)HZ置于(yu)加(jia)水(shui)熱(re)(re)反(fan)(fan)(fan)(fan)應釜(fu)熱(re)(re)器(qi)內,按照規定(ding)(ding)的(de)(de)(de)升溫(wen)(wen)(wen)(wen)(wen)速率(lv)升溫(wen)(wen)(wen)(wen)(wen)至(zhi)所需反(fan)(fan)(fan)(fan)應溫(wen)(wen)(wen)(wen)(wen)度(du)（小(xiao)于(yu)規定(ding)(ding)的(de)(de)(de)使(shi)用(yong)溫(wen)(wen)(wen)(wen)(wen)度(du)）.待反(fan)(fan)(fan)(fan)應結束(shu)將(jiang)其(qi)降溫(wen)(wen)(wen)(wen)(wen)時(shi),也要嚴格(ge)按照規定(ding)(ding)的(de)(de)(de)降溫(wen)(wen)(wen)(wen)(wen)速率(lv)操作(zuo),以(yi)利安quan和(he)(he)水(shui)熱(re)(re)反(fan)(fan)(fan)(fan)應釜(fu)的(de)(de)(de)使(shi)用(yong)壽命(ming).當(dang)確認(ren)腹內溫(wen)(wen)(wen)(wen)(wen)度(du)低于(yu)反(fan)(fan)(fan)(fan)應物(wu)系(xi)(xi)種(zhong)溶劑沸點后(hou)方(fang)(fang)能(neng)(neng)打開釜(fu)蓋進行后(hou)續操作(zuo).每次水(shui)熱(re)(re)反(fan)(fan)(fan)(fan)應釜(fu)使(shi)用(yong)后(hou)要及(ji)時(shi)將(jiang)其(qi)清洗干凈,以(yi)免銹蝕.釜(fu)體(ti)、釜(fu)蓋線密封處(chu)(chu)要格(ge)外(wai)注意清洗干凈,并嚴防將(jiang)其(qi)碰傷損壞.更多相關知識,可以(yi)與(yu)本公司(si)聯系(xi)(xi).